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The overall charge number of the electrode reaction is then n> while the exponential term in the rate constant of the electrode reaction has a form corresponding to a one-electron reaction. If the value of EOf is not known, then the conventional rate constant of the electrode reaction is introduced, kcony = kf'exp(alFE%'/RT), so that Eq. (5.2.48) can be expressed in the form j = - nFkcony exp ( - ~ " ) c i (5.2.49)

grating formation and the possibility of multiple successive recordings evidence the mechanism of grating formation as light-induced mass transport, although affected by the presence of irreversible cross-linking Note that the sol gel materials based on polysiloxane have been known for their durability and good optical quality If functionalized with azobenzene moieties, they exhibit nonlinear optical properties and photoinduced anisotropy There are a few examples of SRG inscribed onto materials (Kim et al, 2006b; Chaput et al, 2000; Frey et al, 2000; Darracq et al, 1998) The gratings could be inscribed only in freshly prepared lms, whereas in aged lms, the cross-linking of the polymer completely hindered SRG formation The ionic sol gel materials (Kulikovska et al, 2008a; Kulikovska et al, 2009) differ by the ionic bonding between the matrix and chromophore Obviously, the presence of ionic groups and interactions affect the lm properties.

If the single-electron mechanism has not been demonstrated to be the rate-controlling process by an independent method, then, in the publication of the experimental results, it is preferable to replace the assumed quantity ocx by the conventional value cm, provided that the charge number of the overall reaction is known (e.g. in an overall two-electron reaction it is preferable to replace 0^ = 0.5 by or = 0.25). If the independence of the charge transfer coefficient on the potential has not been demonstrated for the given potential range, then it is useful to determine it for the given potential from the relation for a cathodic electrode reaction (cf. Eq. 5.2.37):

Management of the BladeRacks is done on a tiered system. Each chassis has a management module built into it, with a management point every 11 blades; each management point talks to higher-level Verari Service Module (VSM) with Verari Command Center (VCC). This tiered approach allows the ability to control over 10,000 blades through one interface.

In these materials, the aging of lms is also accompanied by chemical crosslinking of the matrix, but is much slower The lms had to be either 1-month-old at room conditions or heated at 1501C for 30 min before the SRG formation was suppressed completely Possibly, the freshly prepared lms contain only short polysiloxane oligomers that are suf cient for the formation of good quality lms and effective inscription of SRG The light-induced mass transport is not hindered until a critical degree of cross-linking is accumulated Moreover, it becomes optimal at a certain degree of cross-linking The formation of grating was essentially sped-up by the thermal pretreatment of spin-coated lms: heating the lms at 701C for 30 min led to an increase in the recording rate from 018 to 028/min compared with the freshly prepared lms.

(5 250)

The depth of gratings in pretreated lms was almost three times larger (700 nm) than that in the freshly prepared lms (250 nm) All these results lead to the conclusion that both the rate of grating formation and the achieved relief modulation strongly depend on the lm stiffness and the molecular mobility of the polymer chains If certain mobility is required to.

16

265 A similar relationship is valid for the charge transfer coefficient of the anodic electrode reaction, a,a. The determination of the activation energies of electrode reactions is especially important for the theory of electrode reactions and for study of the relationship between the structure of the reacting substances and the electrode reaction rates. Several descriptions of electrode reaction rates discussed on the preceding pages and the difficulty to standardize electrode potential scales with respect to different temperatures imply several definitions of activation energies of electrode reactions. The easiest way to determine this quantity, for example, for an irreversible cathodic process, employs Eqs (5.2.9), (5.2.10) and (5.2.12) at a constant electrode potential, AH c+anFE A//*

photoconversion, and 0.25 for the back photoreaction. Solvent has a small effect, increasing the trans-cis and decreasing the cis-trans yield as polarity increases (Bortolus and Monti, 1979). Aminoazobenzenes and pseudo-stilbenes isomerize very quickly and can have quantum yields as high as 0.7 0.8.

(5Z51)

Verari offers two blade platforms: the BladeRack and the BladeRack 2. The BladeRack Platforms can be configured with either 66 or 88 dual-processor blade configurations, with support for up to 176 dual-core processors with their patented back-to-back vertical mount design. The BladeRack 2 Platform holds up to 66 blades, supporting as many as 132 dual-core processors. The server blades use both the Intel Xeon and AMD Opteron processors with support for virtual hardware assist.