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Azobenzenes are robust and versatile moieties, and have been extensively investigated as small molecules, pendants on other molecular structures, or incorporated (doped or covalently bound) into a wide variety of amorphous, crystalline, or LC polymeric systems Noteworthy examples include self-assembled monolayers and superlattices (Yitzchaik and Marks, 1996), sol gel silica glasses (Levy and Esquivias, 1995), and biomaterials (Gallot et al, 1996; Willner and Rubin, 1996; Sisido et al, 1991a) A number of small molecules incorporating azobenzene have been synthesized, including crown ethers (Shinkai et al, 1983), cyclodextrins (Jung et al, 1996; Yamamura et al, 1996), proteins such as bacteriorhodopsin (Singh et al, 1996), and three-dimensional (3-D) polycyclics such as cubane (Chen et al, 1997b) and adamantane (Chen et al, 1995) Typically, azo chromophores are embedded in a solid matrix for studies and devices.

This apparently simple expression is actually only conventional; it must be realized that the electrode potential at various temperatures does not differ by only an additive constant when it is referred to different standard reference electrodes, but also by the product of the change in the temperature and the temperature coefficient of this additive constant (see Section 3.1.4). Often, however, the actual value of the activation energy at constant potential AH\ is not of interest, but rather its increase AAi/f, giving the change in the activation energy between two members, e.g. in a homologous series of electroactive substances (see Section 5.9.1). This quantity does not depend on the electrode potential if the charge transfer coefficient a is constant for the electrode process in the studied group of substances. In this case

( 5 2 2 522)) ( dT ) E RT2 RT2 -5 The standard activation energy of the electrode reaction Hi is defined as

As a result, matrix effects are inescapable: the behavior of the chromophore is altered due to the matrix, and in turn, the chromophore alters the matrix (Ichimura, 2000) Although either could be viewed as a nuisance, both are in fact useful: the chromophore can be used as a probe of the matrix (free volume, polarizability, mobility, etc), and when the matrix couples to chromophore motion, molecular motions can be translated to larger length scales Thus, the incorporation strategy is critical to exploiting azobenzene s unique behavior 1131 Amorphous Polymer Thin Films Doping azobenzenes into polymer matrices is a convenient inclusion technique (Birabassov et al, 1998; Labarthet et al, 1998) These guest host systems can be cast or spin-coated from solution mixtures of polymer and azo small molecules, where the azo content in the thin lm is easily adjusted via concentration.

Blades within the BladeRack Platforms can be configured to be client blades. This is accomplished using KVM/IP from Avocent. Verari plans to support dual digital video interface (DVI) per blade by the end of 2006. The addition of a graphics accelerator card on the motherboard is supported.

A typical adsorption process in electrocatalysis is chemisorption, characteristic primarily for solid metal electrodes. The chemisorbed substance is often chemically modified during the adsorption process. Then either the substance itself or some fragment of it is bonded chemically to the electrode. As electrodes mostly have physically heterogeneous surfaces (see Sections 4.3.3 and 5.5.5), the Temkin adsorption isotherm (Eq. 4.3.46) is suitable for characterizing the adsorption. The basic characteristics of electrocatalysis will be demonstrated on several examples, in the first place on the electrode processes of hydrogen,

Although doping leaves the azo chromophores free to undergo photoinduced motion unhindered, it has been found that many interesting photomechanical effects do not couple to the matrix in these systems Furthermore, the azo mobility often leads to instabilities, such as phase separation or microcrystallization Thus, one of the most attractive methodologies for incorporating azobenzene into functional materials is by covalent attachment to polymers The resulting materials bene t from the inherent stability, rigidity, and processability of polymers, in addition to the unusual photoresponsive behavior of the azo moieties Both side-chain and main-chain azobenzene polymers have been prepared (Viswanathan et al, 1999) (Fig 15) Reported synthetic strategies involve either polymerizing azobenzene-functionalized monomers (Ho et al, 1996; Natansohn et al, 1992) or postfunctionalizing.

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