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with m in g s l and tx in s. The theory of voltammetry with rotating disk electrode (RDE) was described in Sections 2.7.2 and 5.4.1. The properties of the voltammetric ultramicroelectrode {UME) were discussed in Sections 2.5.1 and 5.5.1 (Fig. 5.19). The steady-state limiting diffusion current to a spherical UME is Id = 4jtnFDrQc0 while to a hemispherical UME placed on an insulating support Id = 2jtnFDroco (5.5.13) (5.5.12)

copper wire glass tube -

Figure 3.21. Photoinduced contraction of the LCE prepared from Components 17a f. (Inset) Recovery of the contracted LCE at 298 K after irradiation was switched off. Source: Finkelmann and Nishikawa, 2001.

One of the big lessons SAVVIS learned was to be careful with the configuration-management process, including putting procedures in place to handle this new virtualized world, where there is no longer a one-to-one relationship between a box and the environment running on it. They advise new users to pay attention to management systems overall. Their experience is that building virtual machines and virtual environments is the easy part; the management and troubleshooting is harder.

Fig. 5.19 Electrodes used in voltammetry. A dropping mercury electrode (DME). R denotes the reservoir filled with mercury and connected by a plastic tube to the glass capillary at the tip of which the mercury drop is formed. B ultramicroelectrode (UME). The actual electrode is the microdisk at the tip of a Wollaston wire (a material often used for UME) sealed in the glass tube

Figure 3.22. Photographs of photodeformation of azobenzene side-on LCE (a) before irradiation (b) and under irradiation with UV light. Source: Li et al., 2003.

299 For a disk UME situated in the plane of the insulating support Id = 4nFDroco (5.5.14)

17

processes induced by irradiation with UV and visible light, respectively. The monodomain LCE lm bent along the rubbing direction toward the irradiation source, and the bent lm reverted to the initial at state upon exposure to visible light. This bending and unbending behavior was reversible and could be controlled by simply changing the wavelength of the incident light. Furthermore, when the lm was rotated at 901, the bending was again observed along the rubbing direction. These results demonstrate that the bending is anisotropically induced and occurs only along the rubbing direction of the alignment layers. Irradiation with UV light gives rise to the trans cis isomerization of azobenzene moieties and thus destabilization of the nematic phase (decrease in

The non-steady state situation at UME represents a comparatively simple problem at a spherical electrode while it is very difficult to solve in the case of a disk electrode When comparing these three voltammetric electrodes they show different performance with respect to the purpose of their use 1 With a DME, clean surface is quite easy to achieve whereas with the other electrodes a special treatment of the surface is required in order to obtain reproducible results (page 307) Even in solutions containing surfactants, the amount adsorbed at DME can be controlled (cf Section 364) 2 The mass transfer coefficient for both RDE and UME can be varied in a large interval while in the case of DME it is much smaller and also the possibility of changing it is rather restricted 3.

Vis Rubbing direction (c)

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In contrast to DME, the charging of the electric double layer makes no problem with RDE and UME 4 The work with both DME and RDE requires the use of a base (supporting or indifferent) electrolyte, the concentration of which is at least twenty times higher than that of the electroactive species With UME it is possible to work even in the absence of a base electrolyte The ohmic potential difference represents no problem with UME while in the case of both other electrodes it must be accounted for in not sufficiently conductive media The situation is particularly difficult with DME Usually no potentiostat is needed for the work with UME 5 The area of the electrode can easily be measured with DME and RDE while in the case of very small UME it is often difficult to determine 6.

Figure 3.23. Bending and unbending behavior of (a) an LC gel in toluene (b) and an LCE lm in air. (c) Plausible mechanism of the photoinduced bending of LCE lms. Source: Ikeda et al., 2003.