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alignment in response to an external stimulus, the other LC molecules also change their alignment. The energy required to induce an alignment change of only 1 mol% of the LC molecules is enough to bring about the alignment change of the whole system. In other words, a huge ampli cation is possible in LC systems. When a small amount of a photochromic molecule, such as an azobenzene, stilbene, spiropyran, and fulgide derivative, is added to LCs and the resulting guest/host mixture is irradiated to cause photochemical reactions of the photochromic guest molecules, an LC to isotropic phase transition of the mixture can be induced isothermally. Tazuke et al. (1987) reported the rst explicit example of a nematic isotropic phase transition induced by trans cis photoisomerization of an azobenzene guest molecule dispersed in a nematic LC. The photochemically induced phase transitions ( photochemical phase transitions ) are interpreted in terms of a change in the phase transition temperature of LC systems upon accumulation of one isomer of the photochromic guest molecule (Sung et al., 2002; Legge and Mitchell, 1992). The trans form of the

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The study of electrochemical kinetics includes measurement of various electrical data but, at the same time, it needs information on reaction

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291 products and on the situation in the interphase. Thus, electrochemical methodology includes genuine electrochemical methods, analysis of the products of these processes, methods based on interaction of electromagnetic radiation, electrons or other charged species with the electrolysed system or with the electrode itself, etc. Electrochemical methods have been described in a number of excellent monographs (e.g. Bard and Faulkner, Albery, the Southampton Electrochemistry Group, etc., see page 253). Thus, only the general characteristics of these methods will be given here. They mostly provide information on the functional relationships between the current density, electrode potential, time passed since the beginning of the electrolysis and sometimes also the total charge passed through the system. The use of these methods is connected with two main problems: 1. Elimination of the ohmic electric potential difference in the electrolytic cell 2. Selection of a fixed or programmed electric variable The electrode material and its pretreatment considerably influence the course of the electrode process. The importance of non-electrochemical methods is constantly increasing as a result of the development of experimental techniques. 5.5.1 The ohmic electrical potential difference

(CH2)5

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The origin of the ohmic potential difference was described in Section 2.5.2. The ohmic potential gradient is given by the ratio of the local current density and the conductivity (see Eq. 2.5.28). If an external electrical potential difference AV is imposed on the system, so that the current / flows through it, then the electrical potential difference between the electrodes will be AV = Ex - E2 + AV ohm = Ex - E2 + IRt (5.5.1)

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E (c)

where Ex and E2 are the electrode potentials, &Vohm = IRt is the ohmic electrical potential difference and / , is the resistance of the electrolytic cell, measured between the surfaces of the two electrodes. This approach involves the average values of these quantities; the electrode potential and ohmic electrical potential difference values can exhibit local variations in actual systems. In the case of a cylindrical electrolytic cell with electrodes forming bases of the cylinder the ohmic potential difference is AVohm = Ipl/S (5.5.2)

Figure 3.16. Electroclinic effect in ferroelectric LCEs: (a) Chemical structure of sample. (b) Measurement geometry: the beam in the interferometer passes twice through the lm to measure the electrically induced thickness modulation. (c) The viewing angle is turned by 901 around the layer normal compared with that in (b). Source: Lehmann et al., 2001.

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where / is the current, p the resistivity of the electrolyte, / the height and S the cross-section of the cylinder. Electrolytic cells with more diversified forms require more complicated approaches. For a centrosymmetrical

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